4J23
Low resolution crystal structure of the FGFR2D2D3/FGF1/SR128545 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Detector technology | CCD |
| Collection date | 2010-06-11 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.9724 |
| Spacegroup name | P 62 2 2 |
| Unit cell lengths | 210.674, 210.674, 72.512 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.814 - 3.882 |
| R-factor | 0.3243 |
| Rwork | 0.321 |
| R-free | 0.38400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1djs |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.738 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 182.449 | 3.895 |
| High resolution limit [Å] | 3.882 | 3.882 |
| Rmerge | 0.123 | 1.352 |
| Number of reflections | 9212 | |
| <I/σ(I)> | 21.4 | 2.9 |
| Completeness [%] | 100 | |
| Redundancy | 21.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
