4HTX
Crystal structure of PDE2 catalytic domain in complex with BAY60-7550
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-06-27 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 1 |
| Unit cell lengths | 56.260, 73.820, 92.470 |
| Unit cell angles | 109.59, 91.93, 90.88 |
Refinement procedure
| Resolution | 44.160 - 1.900 |
| R-factor | 0.1754 |
| Rwork | 0.173 |
| R-free | 0.22660 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1z1l |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.023 |
| Data reduction software | iMOSFLM |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.160 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 97808 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
