4F2A
Crystal structure of cholestryl esters transfer protein in complex with inhibitors
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-BM |
| Synchrotron site | APS |
| Beamline | 17-BM |
| Detector technology | CCD |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 68.772, 69.915, 187.145 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.880 - 3.110 |
| R-factor | 0.1855 |
| Rwork | 0.183 |
| R-free | 0.23890 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.350 |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 3.100 |
| Rmerge | 0.111 |
| Number of reflections | 12770 |
| Completeness [%] | 76.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
