4BV4
Structure and allostery in Toll-Spatzle recognition
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Collection date | 2012-09-22 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 198.310, 57.110, 70.500 |
Unit cell angles | 90.00, 97.76, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.120 | 2.430 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.080 | 0.780 |
Number of reflections | 24588 | |
<I/σ(I)> | 11.5 | 2.6 |
Completeness [%] | 74.8 | 32.9 |
Redundancy | 3.9 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 15% PEG 8000, 0.1M TRIS PH 7.5, 0.1 M MGCL2 |