4A0K
STRUCTURE OF DDB1-DDB2-CUL4A-RBX1 BOUND TO A 12 BP ABASIC SITE CONTAINING DNA-DUPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-07-30 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 210.650, 78.020, 276.620 |
Unit cell angles | 90.00, 108.50, 90.00 |
Refinement procedure
Resolution | 19.977 - 5.930 |
R-factor | 0.2691 |
Rwork | 0.269 |
R-free | 0.26950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 2HYE AND 3EI2 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.403 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER (MOLREP) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 6.080 |
High resolution limit [Å] | 5.930 | 5.930 |
Rmerge | 0.140 | 0.550 |
Number of reflections | 11289 | |
<I/σ(I)> | 8.1 | 2.41 |
Completeness [%] | 98.5 | 99.9 |
Redundancy | 4.9 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.3 | 100MM TRIS-HCL PH 8.3, 33% PEG 200 |