3ZNP
IN VITRO AND IN VIVO INHIBITION OF HUMAN D-AMINO ACID OXIDASE: REGULATION OF D-SERINE CONCENTRATION IN THE BRAIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS |
Synchrotron site | ALS |
Temperature [K] | 100 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 84.069, 84.069, 189.163 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.980 - 2.400 |
R-factor | 0.2356 |
Rwork | 0.232 |
R-free | 0.30670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2du8 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.170 |
Data reduction software | d*TREK |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.660 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.080 | 0.460 |
Number of reflections | 30588 | |
<I/σ(I)> | 7.7 | 1.9 |
Completeness [%] | 98.5 | 99.5 |
Redundancy | 3.27 | 3.27 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |