Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3ZNI

Structure of phosphoTyr363-Cbl-b - UbcH5B-Ub - ZAP-70 peptide complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2012-10-15
DetectorDECTRIS PILATUS 6M
Spacegroup nameP 1 21 1
Unit cell lengths94.970, 131.800, 122.000
Unit cell angles90.00, 91.92, 90.00
Refinement procedure
Resolution30.540 - 2.210
R-factor0.1767
Rwork0.175
R-free0.21140
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB ENTRIES 3PFV 2ldr 4A49 AND 4AUQ
RMSD bond length0.004
RMSD bond angle0.811
Phasing softwarePHASER
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.5002.270
High resolution limit [Å]2.2102.210
Rmerge0.0600.690
Number of reflections149230
<I/σ(I)>14.22.1
Completeness [%]99.699.9
Redundancy3.43.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
10.1 M BICINE, PH 9.0, 8-11% (W/V) PEG 3350 AND 0.1 M SODIUM FORMATE
10.1 M BICINE, PH 9.0, 8-11% (W/V) PEG 3350 AND 0.1 M SODIUM FORMATE

224201

PDB entries from 2024-08-28

PDB statisticsPDBj update infoContact PDBjnumon