3ZIU
Crystal structure of Mycoplasma mobile Leucyl-tRNA Synthetase with Leu-AMS in the active site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-04 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 202.851, 202.851, 213.922 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 135.760 - 2.070 |
R-factor | 0.16155 |
Rwork | 0.160 |
R-free | 0.19893 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4aq7 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.509 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CCP4 |
Refinement software | REFMAC (5.6.0116) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.000 | 2.120 |
High resolution limit [Å] | 2.070 | 2.070 |
Rmerge | 0.230 | 0.990 |
Number of reflections | 101516 | |
<I/σ(I)> | 18.45 | 2.56 |
Completeness [%] | 100.0 | 99.2 |
Redundancy | 12.4 | 11.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 0.1M BIS-TRIS PH 5.5 0.6M AMMONIUM ACETATE 20% V/V PEG 3350 |