3ZEF
Crystal structure of Prp8:Aar2 complex: second crystal form at 3.1 Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-06 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 125.420, 177.841, 216.601 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 137.450 - 3.100 |
R-factor | 0.22253 |
Rwork | 0.220 |
R-free | 0.26711 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 3SBT 2og4 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.534 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0016) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 137.500 | 3.150 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.160 | 1.300 |
Number of reflections | 97506 | |
<I/σ(I)> | 6.4 | 1.4 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.9 | 7-9% PEG 8000, 100 MM NA-CITRATE PH 7.9, 50-200 MM AMMONIUM SULFATE |