3WZE
KDR in complex with ligand sorafenib
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.99985 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 135.921, 57.357, 52.170 |
| Unit cell angles | 90.00, 94.17, 90.00 |
Refinement procedure
| Resolution | 67.780 - 1.900 |
| R-factor | 0.18771 |
| Rwork | 0.185 |
| R-free | 0.22406 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.469 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 67.780 | 2.150 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.031 | 0.448 |
| Number of reflections | 30435 | |
| Completeness [%] | 95.9 | 97.6 |
| Redundancy | 2.7 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8 | 277 | 10-25% PEG 3350, Na3Citrate, 0.1M Bis-Tris propane, pH 8.0, VAPOR DIFFUSION, temperature 277K |
