3WJ8
Crystal Structure of DL-2-haloacid dehalogenase mutant with 2-bromo-2-methylpropionate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 63 |
Unit cell lengths | 186.309, 186.309, 114.315 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.700 |
R-factor | 0.19561 |
Rwork | 0.187 |
R-free | 0.26863 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.616 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 161.350 |
High resolution limit [Å] | 2.700 |
Number of reflections | 61648 |
Completeness [%] | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | pH 7.5, VAPOR DIFFUSION, temperature 298K |