3VLG
Crystal structure of the W150A mutant LOX-1 CTLD showing impaired OxLDL binding
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2011-02-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.244, 62.244, 76.671 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.170 - 2.300 |
R-factor | 0.1824 |
Rwork | 0.179 |
R-free | 0.24648 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yxk |
RMSD bond length | 0.022 |
RMSD bond angle | 1.815 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.380 |
High resolution limit [Å] | 2.300 | 4.950 | 2.300 |
Rmerge | 0.094 | 0.044 | 0.369 |
Number of reflections | 6945 | ||
<I/σ(I)> | 45.81 | 77.4 | 10.9 |
Completeness [%] | 97.3 | 99.3 | 95.6 |
Redundancy | 13.8 | 12.2 | 14.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 277 | 20% PEG8000, 0.1M sodium citrate, 0.2M ammonium sulfate, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |