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3UMI

X-ray structure of the E2 domain of the human amyloid precursor protein (APP) in complex with zinc

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.2
Synchrotron siteBESSY
Beamline14.2
Temperature [K]100
Detector technologyCCD
Collection date2010-06-04
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.28248
Spacegroup nameP 43
Unit cell lengths39.757, 39.757, 126.425
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution27.440 - 2.400
R-factor0.204
Rwork0.204
R-free0.24500
Structure solution methodSAD
RMSD bond length0.005
RMSD bond angle0.948
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareSHARP
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]27.4402.530
High resolution limit [Å]2.4002.400
Number of reflections7453
Completeness [%]96.889
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.42930.1 mM HEPES, 1 M sodium acetate, 10 mM MgCl2, 50 mM CdSO4, pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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