Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-29 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9791532 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 70.640, 70.640, 125.880 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.010 - 1.950 |
R-factor | 0.1597 |
Rwork | 0.157 |
R-free | 0.20270 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.718 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.980 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 27293 | |
<I/σ(I)> | 52.18 | 3.46 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.3 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.2 M DI-AMMONIUM HYDROGEN CITRATE, 16% PEG3350, 2MM HYGROMYCIN B, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 298K |