3SL9
X-ray structure of Beta catenin in complex with Bcl9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-20 |
Detector | ADSC QUANTUM 4r |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 160.890, 80.700, 87.940 |
Unit cell angles | 90.00, 102.00, 90.00 |
Refinement procedure
Resolution | 29.430 - 2.200 |
R-factor | 0.197 |
Rwork | 0.194 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2gl7 |
RMSD bond length | 0.024 |
RMSD bond angle | 1.969 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.070 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.050 | 0.050 |
Number of reflections | 54333 | |
<I/σ(I)> | 17.1 | 17.1 |
Completeness [%] | 97.2 | 97.2 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 298 | 0.12M ethylene glycol, 1M MES 62% MES, 1M Imidazol 38%, 10% PEG 4K, 20% glycerol, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |