3SH9
Crystal structure of fluorophore-labeled beta-lactamase PenP in complex with cefotaxime
Replaces: 3KGNExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Collection date | 2008-07-15 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.386, 91.626, 66.008 |
Unit cell angles | 90.00, 104.50, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.900 |
R-factor | 0.2 |
Rwork | 0.197 |
R-free | 0.24634 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4blm |
RMSD bond length | 0.012 |
RMSD bond angle | 1.615 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.800 |
High resolution limit [Å] | 1.900 |
Number of reflections | 39490 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | PEG4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |