3RY6
Complex of fcgammariia (CD32) and the FC of human IGG1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-04-01 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 153.380, 255.550, 58.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.710 - 3.800 |
R-factor | 0.252 |
Rwork | 0.252 |
R-free | 0.42600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e4k |
RMSD bond angle | 1.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.940 |
High resolution limit [Å] | 3.800 | 3.800 |
Number of reflections | 11766 | |
<I/σ(I)> | 10.8 | 3.78 |
Completeness [%] | 98.7 | 99.7 |
Redundancy | 5 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.4 | 20% (W/V) PEG 3350, 5MM TRIS, 0.15M NACL, 2MM MOPS, 0.2M TRI-POTASSIUM ACETATE, PH 7.40, VAPOR DIFFUSION, TEMPERATURE 291.0K |