3RL0
Truncated SNARE complex with complexin (P1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2010-04-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9797 |
Spacegroup name | P 1 |
Unit cell lengths | 53.745, 127.357, 142.725 |
Unit cell angles | 107.49, 90.01, 90.05 |
Refinement procedure
Resolution | 30.000 - 3.800 |
R-factor | 0.308 |
Rwork | 0.306 |
R-free | 0.34500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.035 |
RMSD bond angle | 1.011 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.940 |
High resolution limit [Å] | 3.800 | 3.800 |
Completeness [%] | 83.5 | 80.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 294 | 13-15% polyethyleneglycol (PEG) 5000MME, 0.2 M ammonium sulfate, 0.01 M EDTA, and 0.1 M Tris pH 7.5, VAPOR DIFFUSION, temperature 294K |