Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Detector technology | CCD |
Collection date | 2008-06-11 |
Wavelength(s) | 1.000 |
Spacegroup name | P 3 |
Unit cell lengths | 120.860, 120.860, 93.425 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.660 - 2.500 |
Rwork | 0.227 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1iqa |
RMSD bond length | 0.010 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.660 |
High resolution limit [Å] | 2.500 |
Number of reflections | 52575 |
<I/σ(I)> | 31.4 |
Redundancy | 10.46 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 5.6 | 298 | 100mM trisodium citrate, 1.2M ammonium sulfate, pH 5.6, microbatch, temperature 298K |