3PZE
JNK1 in complex with inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-02-15 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.586, 71.378, 106.731 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.330 - 2.000 |
R-factor | 0.206 |
Rwork | 0.204 |
R-free | 0.23960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.800 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 25419 | |
Completeness [%] | 96.7 | 94.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7 | 298 | 15% PEG2000 MME, 100 mM HEPES, 10 mM DTT, pH 7, EVAPORATION, temperature 298K |