3PPJ
Human B-Raf Kinase in Complex with a Furopyridine Inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-07-15 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 100.540, 100.540, 162.110 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.480 - 3.700 |
R-factor | 0.251 |
Rwork | 0.250 |
R-free | 0.27200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.100 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.930 |
High resolution limit [Å] | 3.700 | 3.700 |
Number of reflections | 9357 | |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | PEG 3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |