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3PMX

Ligand-binding domain of GluA2 (flip) ionotropic glutamate receptor in complex with an allosteric modulator

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2008-09-30
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.54178
Spacegroup nameP 21 21 2
Unit cell lengths64.240, 88.170, 47.345
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.730 - 1.870
R-factor0.22086
Rwork0.218
R-free0.28142
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.014
RMSD bond angle1.442
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.7301.920
High resolution limit [Å]1.8701.870
Rmerge0.661
Number of reflections21208
<I/σ(I)>17.31.9
Completeness [%]92.986.5
Redundancy4.44
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP427718% PEG 4000, 50mM Lithium Sulphate, 2.5% Glycerol, 100mM Sodium Cacodylate pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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