3MVJ
Human cyclic AMP-dependent protein kinase PKA inhibitor complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.163, 120.828, 162.415 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.750 - 2.490 |
R-factor | 0.21671 |
Rwork | 0.212 |
R-free | 0.30436 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 1.816 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.350 | 2.590 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.158 | 0.683 |
Number of reflections | 41833 | |
<I/σ(I)> | 6.9 | |
Completeness [%] | 98.0 | 96.9 |
Redundancy | 7.1 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |