3KXU
Crystal structure of human ferritin FTL498InsTC pathogenic mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 151.355, 151.355, 151.355 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.780 - 1.850 |
R-factor | 0.18031 |
Rwork | 0.179 |
R-free | 0.21078 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ffx |
RMSD bond length | 0.014 |
RMSD bond angle | 1.244 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.780 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.075 | 0.407 |
Number of reflections | 25503 | |
<I/σ(I)> | 5.8 | 2 |
Completeness [%] | 98.3 | 98.3 |
Redundancy | 5.1 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 293 | 0.25M CADMIUM SULFATE, 0.1M HEPES, 0.96M SODIUM ACETATE, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |