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3K43

Crystal structure of sCD-MPR mutant E19Q/K137M pH 6.5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]98
Detector technologyIMAGE PLATE
Collection date2009-04-15
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.54
Spacegroup nameI 4
Unit cell lengths102.978, 102.978, 99.818
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution27.460 - 2.000
Rwork0.165
R-free0.19900
Structure solution methoddifference fourier
Starting model (for MR)3k42
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.070
High resolution limit [Å]2.0004.3102.000
Rmerge0.0680.0350.413
Number of reflections35223
<I/σ(I)>15.2
Completeness [%]99.797.9100
Redundancy5.75.95.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52920.1M sodium cacodylate, 3M ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K

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