3K22

Glucocorticoid Receptor with Bound alaninamide 10 with TIF2 peptide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2006-12-15
Detector	ADSC QUANTUM 210
Wavelength(s)	1.0
Spacegroup name	P 61
Unit cell lengths	127.597, 127.597, 78.230
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.850 - 2.100
R-factor	0.214
Rwork	0.211
R-free	0.25500
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.197
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	REFMAC

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	1.860
High resolution limit [Å]	1.800	3.880	1.800
Rmerge	0.039	0.017
Number of reflections	41085
<I/σ(I)>	14.8
Completeness [%]	95.2	89	87.8
Redundancy	2	2.1	1.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1