3JSI

Human phosphodiesterase 9 in complex with inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E SUPERBRIGHT
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2009-05-10
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	P 41 21 2
Unit cell lengths	104.099, 104.099, 271.040
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.650 - 2.720
R-factor	0.205
Rwork	0.205
R-free	0.21820
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	3dyn
RMSD bond length	0.008
RMSD bond angle	0.970
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	BUSTER (2.9.2)
Refinement software	BUSTER (2.9.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.700
Number of reflections	26056

Crystallization Conditions

crystal ID	method	pH	temperature	details
1