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3HY6

Structure of human MTHFS with ADP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2009-03-10
DetectorADSC QUANTUM 315r
Wavelength(s)0.979
Spacegroup nameC 2 2 21
Unit cell lengths48.511, 145.221, 59.655
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution46.090 - 2.100
R-factor0.21728
Rwork0.215
R-free0.25527
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3hxt
RMSD bond length0.011
RMSD bond angle1.280
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.4.0066)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]72.5502.100
High resolution limit [Å]2.1002.000
Number of reflections12552
Completeness [%]99.399.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.6298100mM HEPES, pH6.6, 20mM MgCl2.6H2O, 20mM NiCl2.6H2O, 20% (w/v) PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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