3GXP

Crystal structure of acid-alpha-galactosidase A complexed with galactose at pH 4.5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Spacegroup name	P 32 2 1
Unit cell lengths	89.510, 89.510, 215.927
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	38.150 - 2.200
R-factor	0.204
Rwork	0.201
R-free	0.26500
RMSD bond length	0.020
RMSD bond angle	2.049
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	76.600
High resolution limit [Å]	2.200
Number of reflections	42395

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION			vapor diffusion