3FWC
Sac3:Sus1:Cdc31 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-08-30 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.590, 122.710, 128.710 |
Unit cell angles | 90.00, 95.75, 90.00 |
Refinement procedure
Resolution | 19.924 - 2.700 |
R-factor | 0.214 |
Rwork | 0.211 |
R-free | 0.26460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fwb |
RMSD bond length | 0.006 |
RMSD bond angle | 0.867 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.114 | 0.782 |
Number of reflections | 61904 | |
<I/σ(I)> | 2.8 | 2.8 |
Completeness [%] | 99.1 | 99.1 |
Redundancy | 10.8 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | unbuffered 16% PEG4K, 20% glycerol, 0.2 M Am sulph. See publication for complete details, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 291K |