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3FGU

Catalytic complex of Human Glucokinase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2008-11-21
DetectorPSI PILATUS 6M
Wavelength(s)1.0001
Spacegroup nameP 21 21 21
Unit cell lengths65.880, 82.120, 86.830
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.150
R-factor0.19977
Rwork0.197
R-free0.25529
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3f9m
RMSD bond length0.011
RMSD bond angle1.267
Data scaling softwareSCALA
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0002.270
High resolution limit [Å]2.1502.150
Rmerge0.0760.330
Number of reflections22231
<I/σ(I)>17.23.1
Completeness [%]84.584.8
Redundancy3.62
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5293PEG 4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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