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3BA0

Crystal structure of full-length human MMP-12

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsOXFORD DIFFRACTION ENHANCE ULTRA
Temperature [K]100
Detector technologyCCD
Collection date2006-11-25
DetectorOXFORD ONYX CCD
Wavelength(s)1.5418
Spacegroup nameC 1 2 1
Unit cell lengths135.037, 60.148, 59.611
Unit cell angles90.00, 90.74, 90.00
Refinement procedure
Resolution30.700 - 3.000
R-factor0.24339
Rwork0.236
R-free0.31900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1y93 1su3
RMSD bond length0.049
RMSD bond angle4.271
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.7003.160
High resolution limit [Å]3.0003.000
Rmerge0.1500.430
Number of reflections9308
<I/σ(I)>4.91.8
Completeness [%]97.897.7
Redundancy4.84.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP82980.1M Tris-HCl, 30% PEG8000, 200mM acetohydroxamic acid, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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