3AT4

Crystal structure of CK2alpha with pyradine derivertive

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-17A
Synchrotron site	Photon Factory
Beamline	BL-17A
Temperature [K]	95
Detector technology	CCD
Collection date	2008-11-11
Detector	ADSC QUANTUM 4
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	51.264, 77.305, 79.226
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.660 - 2.200
Rwork	0.242
R-free	0.25100
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2zjw
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	CNX

Data quality characteristics

	Overall
Low resolution limit [Å]	38.660
High resolution limit [Å]	2.200
Number of reflections	16647
Completeness [%]	99.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	277	25% ethyleneglycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K