Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-10-29 |
| Detector | ADSC QUANTUM 210r |
| Wavelength(s) | 0.9791532 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 70.640, 70.640, 125.880 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.010 - 1.950 |
| R-factor | 0.1597 |
| Rwork | 0.157 |
| R-free | 0.20270 |
| Structure solution method | SAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.718 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.980 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Number of reflections | 27293 | |
| <I/σ(I)> | 52.18 | 3.46 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 10.3 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.2 M DI-AMMONIUM HYDROGEN CITRATE, 16% PEG3350, 2MM HYGROMYCIN B, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
