Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Detector technology | CCD |
| Collection date | 2008-06-11 |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 3 |
| Unit cell lengths | 120.860, 120.860, 93.425 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.660 - 2.500 |
| Rwork | 0.227 |
| R-free | 0.24900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1iqa |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.700 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.660 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 52575 |
| <I/σ(I)> | 31.4 |
| Redundancy | 10.46 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 5.6 | 298 | 100mM trisodium citrate, 1.2M ammonium sulfate, pH 5.6, microbatch, temperature 298K |
