3Q2H
Adamts1 in complex with N-hydroxyformamide inhibitors of ADAM-TS4
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E DW |
| Temperature [K] | 100 |
| Collection date | 2007-01-04 |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.859, 63.328, 110.844 |
| Unit cell angles | 90.00, 91.24, 90.00 |
Refinement procedure
| Resolution | 27.700 - 2.330 |
| R-factor | 0.23928 |
| Rwork | 0.236 |
| R-free | 0.29660 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jih |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.486 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.010 | 2.410 |
| High resolution limit [Å] | 2.300 | 2.330 |
| Number of reflections | 29956 | |
| Completeness [%] | 93.9 | 99.9 |
| Redundancy | 4.2 | 4.75 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
