3JSI
Human phosphodiesterase 9 in complex with inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E SUPERBRIGHT |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2009-05-10 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 104.099, 104.099, 271.040 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.650 - 2.720 |
| R-factor | 0.205 |
| Rwork | 0.205 |
| R-free | 0.21820 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 3dyn |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.970 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | BUSTER (2.9.2) |
| Refinement software | BUSTER (2.9.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 26056 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
