3GXP
Crystal structure of acid-alpha-galactosidase A complexed with galactose at pH 4.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 89.510, 89.510, 215.927 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.150 - 2.200 |
R-factor | 0.204 |
Rwork | 0.201 |
R-free | 0.26500 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.049 |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 76.600 |
High resolution limit [Å] | 2.200 |
Number of reflections | 42395 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | vapor diffusion |