3A6P
Crystal structure of Exportin-5:RanGTP:pre-miRNA complex
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-12-12 |
| Detector | Bruker DIP-6040 |
| Wavelength(s) | 0.9000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 71.157, 304.667, 89.230 |
| Unit cell angles | 90.00, 110.79, 90.00 |
Refinement procedure
| Resolution | 39.840 - 2.920 |
| R-factor | 0.25061 |
| Rwork | 0.247 |
| R-free | 0.31242 |
| Structure solution method | MAD |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.828 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.900 |
| Number of reflections | 74959 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
