Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL26B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL26B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-11-14 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9790, 0.9793, 0.9640 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 74.506, 74.506, 146.524 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.840 - 2.100 |
| R-factor | 0.1999 |
| Rwork | 0.199 |
| R-free | 0.22529 |
| Structure solution method | MAD |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.723 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 28345 | |
| <I/σ(I)> | 21.1476 | 4.223 |
| Completeness [%] | 99.9 | 99.4 |
| Redundancy | 9.882 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | Ammonium sulfate, PEG, pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
