2Z3Q

Crystal structure of the IL-15/IL-15Ra complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2006-12-10
Detector	ADSC QUANTUM 315
Spacegroup name	P 21 21 2
Unit cell lengths	78.444, 120.012, 49.459
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.550 - 1.850
R-factor	0.20479
Rwork	0.202
R-free	0.25216
Structure solution method	SAD
RMSD bond length	0.018
RMSD bond angle	1.714
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHENIX
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.920
High resolution limit [Å]	1.850	1.850
Rmerge	0.069	0.380
Number of reflections	39742
<I/σ(I)>	26.38	2.52
Completeness [%]		86.1
Redundancy	9.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1