2YPA
Structure of the SCL:E47:LMO2:LDB1 complex bound to DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 102.966, 141.044, 148.793 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.150 - 2.800 |
R-factor | 0.22614 |
Rwork | 0.224 |
R-free | 0.26945 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.979 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX (AUTOSOL) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.100 | 0.870 |
Number of reflections | 16249 | |
<I/σ(I)> | 11 | 1.2 |
Completeness [%] | 96.3 | 0.9 |
Redundancy | 3.9 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 5 % (V/V) 2-METHYL-2, 4-PENTANEDIOL (MPD), 40 MM MAGNESIUM CHLORIDE, 50 MM SODIUM CACODYLATE PH 6.0 AND 2MM GLUTATHIONE |