2Y0I
FACTOR INHIBITING HIF-1 ALPHA IN COMPLEX WITH TANKYRASE-2 (TNKS2) FRAGMENT PEPTIDE (21-MER)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-14 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 86.490, 86.490, 146.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.940 - 2.280 |
R-factor | 0.2296 |
Rwork | 0.230 |
R-free | 0.24830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h2k |
RMSD bond length | 0.008 |
RMSD bond angle | 1.329 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.340 | 2.340 |
High resolution limit [Å] | 2.280 | 2.280 |
Rmerge | 0.050 | 0.770 |
Number of reflections | 45166 | |
<I/σ(I)> | 23.9 | 3.1 |
Completeness [%] | 99.6 | 98.3 |
Redundancy | 9.3 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 1.6M AMMONIUM SULPHATE, 6% PEG 400, 0.1M HEPES PH 7.5 . |