2XZO
Upf1 helicase - RNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-03-06 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 77.066, 101.896, 112.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.184 - 2.395 |
R-factor | 0.1947 |
Rwork | 0.193 |
R-free | 0.23290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wjv |
RMSD bond length | 0.007 |
RMSD bond angle | 1.024 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.180 | 2.520 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.090 | 0.590 |
Number of reflections | 35441 | |
<I/σ(I)> | 14.5 | 3.3 |
Completeness [%] | 99.8 | 98.5 |
Redundancy | 6.2 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 100 MM SODIUM ACETATE PH 4.6, 20 MM CACL2, 15% MPD |