2VWF
Grb2 SH3C (2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2007-11-08 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 41.166, 41.166, 107.915 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.650 - 1.580 |
R-factor | 0.18951 |
Rwork | 0.188 |
R-free | 0.21907 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vvk |
RMSD bond length | 0.017 |
RMSD bond angle | 1.597 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.640 |
High resolution limit [Å] | 1.580 | 1.580 |
Rmerge | 0.010 | 1.000 |
Number of reflections | 8066 | |
<I/σ(I)> | 26.7 | 2.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 19.5 | 19.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 2M TRI-AMMONIUM CITRATE, 0.1M BIS-TRIS PROPANE PH7, pH 7.0 |