2VUZ
Crystal structure of Codakine in complex with biantennary nonasaccharide at 1.7A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 32.163, 100.197, 95.738 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.130 - 1.700 |
R-factor | 0.204 |
Rwork | 0.202 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vuv |
RMSD bond length | 0.018 |
RMSD bond angle | 1.763 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.600 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.080 | 0.380 |
Number of reflections | 17204 | |
<I/σ(I)> | 5.3 | 2 |
Completeness [%] | 98.6 | 99.3 |
Redundancy | 5.6 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2M LITHIUM SULFATE IN 100 MM SODIUM ACETATE PH 7.5 WITH 15% PEG 4000 |