2VC9

Family 89 Glycoside Hydrolase from Clostridium perfringens in complex with 2-acetamido-1,2-dideoxynojirmycin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113.15
Spacegroup name	P 61
Unit cell lengths	90.960, 90.960, 252.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.700 - 2.360
R-factor	0.205
Rwork	0.203
R-free	0.24600
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.157
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.830
High resolution limit [Å]	2.360
Rmerge	0.130
Number of reflections	42780
Completeness [%]	90.7
Redundancy	3.27

Crystallization Conditions

crystal ID	method	pH	temperature	details
1