Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

2RH1

High resolution crystal structure of human B2-adrenergic G protein-coupled receptor.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-B
Synchrotron siteAPS
Beamline23-ID-B
Temperature [K]78
Detector technologyCCD
Collection date2007-06-22
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1.03321
Spacegroup nameC 1 2 1
Unit cell lengths106.318, 169.240, 40.154
Unit cell angles90.00, 105.62, 90.00
Refinement procedure
Resolution19.950 - 2.400
R-factor0.198
Rwork0.196
R-free0.23200
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB entries 1U19 2lzm
RMSD bond length0.013
RMSD bond angle1.500
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]20.00020.0002.500
High resolution limit [Å]2.40010.0002.400
Rmerge0.1270.0660.678
Number of reflections265063333060
<I/σ(I)>9.6223.22.2
Completeness [%]99.287.499.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1LIPIDIC MESOPHASE6.7529330-35% v/v PEG 400, 0.1-0.2 M Na2SO4, 0.1 M Bis-tris propane pH 6.5-7.0, 5-7% 1,4-Butanediol, 8-10% Cholesterol, 52-50% Monoolein, pH 6.75, LIPIDIC MESOPHASE, temperature 293K
1LIPIDIC MESOPHASE6.7529330-35% v/v PEG 400, 0.1-0.2 M Na2SO4, 0.1 M Bis-tris propane pH 6.5-7.0, 5-7% 1,4-Butanediol, 8-10% Cholesterol, 52-50% Monoolein, pH 6.75, LIPIDIC MESOPHASE, temperature 293K

225158

PDB entries from 2024-09-18

PDB statisticsPDBj update infoContact PDBjnumon