2QFA
Crystal structure of a Survivin-Borealin-INCENP core complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Wavelength(s) | 0.99 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.467, 78.793, 100.017 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.000 - 1.400 |
R-factor | 0.186 |
Rwork | 0.184 |
R-free | 0.20200 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.326 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXS |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.000 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.060 | 0.392 |
Number of reflections | 64114 | |
<I/σ(I)> | 15.2 | 2.6 |
Completeness [%] | 96.0 | 80.1 |
Redundancy | 5.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 293 | 50mM MES pH6, 10% PEG3350, VAPOR DIFFUSION, temperature 293K |