2NRU
Crystal structure of IRAK-4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 145.303, 141.292, 88.423 |
Unit cell angles | 90.00, 125.80, 90.00 |
Refinement procedure
Resolution | 90.290 - 2.000 |
R-factor | 0.23665 |
Rwork | 0.233 |
R-free | 0.29880 |
Structure solution method | SAD |
RMSD bond length | 0.021 |
RMSD bond angle | 2.107 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 90.290 |
High resolution limit [Å] | 2.000 |
Number of reflections | 92544 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.4 | 293 | 2.6 - 2.9 M ammonium sulfate, PH 6.4-7.9, EVAPORATION, temperature 293K |